Synthesis and Characterization a New 1,3-Diazepine Compounds from New Bis 4-Amino-3-Mercpto-1,2,4-Triazole Derivatives

Authors

  • Atyaf AQ Younus
  • Nasreen R Jber

Keywords:

1,3-Diazepine, 1,2,4-Traiazole, Schiff`s bases

Abstract

Compounds with two triazole rings IVa,b were synthesized through the reaction of diacid hydrazide firstly with CS2/KOH, and secondly with excess of hydrazine hydrate. The one-step reaction of isatin with benzylidene benzeneamine (S1–S10) in ethanol gave 2-Ar-3- Ar'[3,4b][1,3]benzodiazepine-4,5-diones (D1-D10) in good yields. The products were characterized using FTIR, 1HNMR spectroscopy and CHN elemental analyses.

 

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Published

2017-06-01

Issue

Vol. 20 No. 2 (2017): June

Section

Articles

How to Cite

(1)
Synthesis and Characterization a New 1,3-Diazepine Compounds from New Bis 4-Amino-3-Mercpto-1,2,4-Triazole Derivatives. ANJS 2017, 20 (2).