SYNTHESIS AND STUDY OF NEW METAL COMPLEXES DERIVED FROM 5-AMINO-3[4'-PNITRO PHENYL-THIOSEMICARBAZIDO]-1,2,4- THIADIAZOLE
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Abstract
The new ligand 5-amino -3-[4'-P-nitrophenyl thiosemicarbazido]-1,2,4-Thiodiazole(L) was prepared a long with its metal complexes with the selected ions Cr(III) ,Mn(II) ,Co(II), Ni(II), Cu(II) and Zn(II).The prepared complexes were elucidated by microelemental analysis (C.H.N.M), spectral methods (UV- vissible) and (FT.IR ),and other physical measurements (molar conductance in 10-3 M solution of (DMF), magnetic susceptibility for solid complexes and studied in solution using molar ratio(M:L) in ethanolic solution, Further more the stability of complexes in solutions were estimated via determination of stability constant Ks by spectrophotometric method.
Published
2018-08-08
How to Cite
Albaity, S. M. M., & Al-Obaidi, N. J. (2018). SYNTHESIS AND STUDY OF NEW METAL COMPLEXES DERIVED FROM 5-AMINO-3[4’-PNITRO PHENYL-THIOSEMICARBAZIDO]-1,2,4- THIADIAZOLE. Al-Nahrain Journal of Science, 12(2), 15-24. Retrieved from https://anjs.edu.iq/index.php/anjs/article/view/1233
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